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Gas Chromatography-Mass Spectrometer

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Introduction:
The product integrates the functions of instrument tuning, data processing, and data analysis to improve the operational performance of the instrument and make research work more efficient.

⚠This item is not returnable. View return policy

Description

Gas Chromatography-Mass Spectrometer

Application:

Food safety: pesticide residues, flavors, fragrances, additives, packaging materials

Environmental monitoring: air, water quality, soil, solid waste

Industrial manufacturing: textiles, cosmetics, electrical and electronic products, plastic products, biomedicine

Petrochemical: refinery, chemical plant

Public security system: criminal investigation, explosives, drugs, physical evidence identification

 

Feature:

1.The temperature and pressure control precision of gas chromatography has reached the international first-class level.

2.The wide temperature RF power supply can adapt to various laboratory environments and perform more stably.

3.High-precision all-metal quadrupole, ensuring good resolution,

4.Quadrupole mass analyzer with pre-quadrupole, more resistant to pollution,

Electron multiplier with high- energy dynode, guaranteeing excellent sensitivity.

6.The high-performance turbomolecular pump ensures the high vacuum environment of mass spectrometry.

7.The inert ion source has high ionization efficiency, and the dual filament design provides double the service time.

8.Autosampler, purge and trap, thermal desorption, and headspace sampler can be configured according to the state of the sample.

Gas Chromatography-Mass Spectrometer

Wide-temperature RF power supply can better adapt to various laboratory environments and provide better stability.

Gas Chromatography-Mass Spectrometer

The high-temperature inert ion source ionizes efficiently, reduces pollution, and is equipped with two long-life filaments, providing double the service time.

Gas Chromatography-Mass Spectrometer

High-precision all-metal quadrupole to ensure good mass spectral resolution.

Gas Chromatography-Mass Spectrometer

The imported high- performance turbomolecular pump is adopted, with high pumping speed, stable operation and long life, providing an excellent vacuum environment for mass spectrometry.

Gas Chromatography-Mass Spectrometer

 

Reliable analysis results come from technology that strives for perfection

BK-GCMS9600A has been repeatedly tested with 24 injections of OFN samples, and the RSD is only 0.995%.

Parameter:

Model BK-GCMS9600A
Standard Configuration MS Unit:

1.GCMS9700A single quadrupole mass spectrometer with workstation software* 1

2. Turbo molecular pump 90l/s* 2

3. Vacuum pump 4m3/h* 1

4. Inert EI ion source* 1

GC Unit:

5.A91PLUS gas chromatograph host, pressure control accuracy 0.001psi *1

6. Split/splitless inlet *1

7. GC Starter Kit

8. MS ion source maintenance kit

Option 24-postions liquid autosampler

Column

Power Supply 220V±10%,50Hz
Package Size(L*W*H) GC: 960*760*700mm

MS: 780*520*650mm

Pump: 600*300*220mm

Gross Weight GC: 50kg

MS:55Kg

Pump:22kg

Application Examples

 

Environmental Detection Application Example

 

Test for 16 PAHs Samples

 

Testing Method

Instrument used for detection: BK-GCMS9600A

Column: DB- 5MS, 30m X 0.25mm X 0.25 μ m

Oven: 50°C (2min) 25°C/min 200°C (0min) 8C/min 300°C (5.5min)

Source temperature: 270°C

Transfer line temperature: 280°C

Injection volume: 1.0μL

Solvent delay: 5min

Scan mode: SIM mode; Scan mode

Gas Chromatography-Mass Spectrometer

SIM mode chromatographic spectrum of polycyclic aromatic hydrocarbons

 

Test for 57 VOCs in water

 

Testing Method

Instrument used for test: BK-GCMS9600A ; CDS7000 PT

Column: DB-624, 30m X 0.25mm X 1.4μm

Oven: 35°C (2min) 5°C/min;120°C (0min) 10°C/min;220°C (2min)

Source temperature: 240°C

Transfer line temperature: 250°C

Injection volume: 5.0mL aqueous solution

Column flow: 1 .0ml /min

Solvent delay: 2.0min

Scan mode: SIM mode

Gas Chromatography-Mass Spectrometer

SIM mode chromatographic spectrum of 57 VOCs in water

Testing Examples In The Food Industry

 

Pesticide residue detection

 

Testing Method

Instrument used for test: BK-GCMS9600A

Column: DB-1701, 30m X 0.25mm X 0.25 μm

Oven: 40°C (1min) 30°C/min;130°C (0min) 5°C /min;250° (0min) 10°C/min 300°C (5min)

Source temperature: 240°C

Transfer line temperature: 280°C

Solvent delay: 2.0min

Scan mode: SIM mode

Gas Chromatography-Mass Spectrometer

Difenoconazole (cis and trans) Mass lon Chromatogram

Gas Chromatography-Mass Spectrometer

Fluoroamide Mass lon Chromatogram

Plasticizer Testing

 

Testing Method

Instrument used for test: BK-GCMS9600A

Column: DB-5MS, 30m X 0.25mm X 0.25 μm

Oven: 80°C (0.5min) 25°C/min 300°C (4.5min)

Injection volume: 1μL

Source temperature: 270°C

Transfer line temperature: 280°C

Solvent delay: 3min

Inlet mode: Split inlet, split ratio 20:1

Scan mode: SIM mode

Gas Chromatography-Mass Spectrometer

Plasticizer DBP, BBP, DEHP m/z= =149 MIC

Example Of Drug Detection In Public Security Department

 

Example of drug detection

 

Testing Method

Instrument used for test: BK-GCMS9600A

Column: DB- 5MS, 30m X 0.25mm X 0.25 μm

Inlet temperature: 280°C

Oven: 60°C (0min) 15°C/min 280C (15min)

Source temperature: 240°C

Transfer line temperature: 250°C

Column flow (constant): 1.0mL/min

Inlet mode: Split inlet, split ratio 20:1

Solvent delay: 3.0min

Scan mode: Full scan, SIM

Scan mass range: 40 – 500amu

Gas Chromatography-Mass Spectrometer

Methamphetamine mass ion chromatogram

Gas Chromatography-Mass Spectrometer

Methamphetamine spectral library search

Gas Chromatography-Mass Spectrometer

Total ion chromatogram and mass spectrum of 3 fentanyl samples (1 ppm)

Methamphetamine spectral library search

The test results show that the gas chromatography-mass spectrometer is used in the detection of drug methamphetamine samples, with accurate results and simple operation method. Meet the inspection and identification requirements of the public security department for methamphetamine drugs.

For the detection of other drug samples, such as the test of fentanyl mixed standard at 1ppm concentration, the mass spectrum peak shape is good, the separation effect is obvious, the result is stable and the reliability is high.

Examples Of Pesticide Sample Detection

 

Determination of organochlorine pesticide residues in solid waste

 

Testing Method

Instrument used for test: BK-GCMS9600A

Column: DB-17MS, 30m X 0.25mm X 0.25 μm

Inlet mode: Pulsed splitless mode

Inlet temperature: 270°C

Oven: 40°C (1min) 30°C/min;130°C (0min) 5°C/min;225°C (0min) 10°C/min; 280°C (5min)

Source temperature: 280°C

Transfer line temperature: 280°C

Solvent delay: 5.0min

Scan mode: Full scan mode; SIM mode

Gas Chromatography-Mass Spectrometer

Total ion chromatogram of 19 organophosphorus pesticides

 

1. Dichlorvos

2. Procymidone

3. Dementon-O+S

4. Ethoprophos

5. Thionazin

6. Sulfotep

7. Thimet

8. Diazinon

9. Disulfoton

10. Dimethoate

11. Fenchlorphos

12. Parathion-methyl

13. Merphos

14. Triadimefon

15. Chlorpyrifos

16. Fipronil

17. Piperonyl butoxide

1 8. Thiodan sulfate

19. Bromopropylate

 

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Item: Gas Chromatography-Mass Spectrometer